Preparation,Characterization and Electrical Properties Studies of Nano Sized Cerium Neodymium Doped Magnesium Ferrite
International Journal of Electronics and Communication Engineering |
© 2018 by SSRG - IJECE Journal |
Volume 5 Issue 3 |
Year of Publication : 2018 |
Authors : S.K.A. Ahamed Kandu Sahib, M.Sharon Eloise Violet, T.Sheeba, S.Usha Rani |
How to Cite?
S.K.A. Ahamed Kandu Sahib, M.Sharon Eloise Violet, T.Sheeba, S.Usha Rani, "Preparation,Characterization and Electrical Properties Studies of Nano Sized Cerium Neodymium Doped Magnesium Ferrite," SSRG International Journal of Electronics and Communication Engineering, vol. 5, no. 3, pp. 10-13, 2018. Crossref, https://doi.org/10.14445/23488549/IJECE-V5I3P103
Abstract:
Nano crystalline magnesium Cerium Neodymium ferrite with general formula MgCex Ndy Fe2-x-y O4 (where x = 0.04, 0.06, 0.08, 0.10 and y=0.03,0.04,0.05,0.06) were prepared through sol-gel route from high purity nitrates of M agnesium (M g), Cerium(Ce), Neodymium(Nd) and Iron. The samples were sintered in microwave furnace and then characterized by XRD and SEM techniques. X-ray diffraction measurements confirmed the Nano size and formation of single phase cubic spinel structure of Magnesium ferrite. It was found that the lattice constant decreases with the increase in Nd3+Ce3+ concentration and the crystalline size of the samples was lying in the range of 53.22 – 53.74 nm, which was confirmed from the XRD studies. SEM studies show that the grain size of the samples decreases with the increase in Nd3+ Ce3+ content. This concludes that Nd3+ , Ce3+ occupies B-site.. The dielectric studies confirm the electrical behaviour and used to understand the electromagnetic properties of these nano ferrite materials. The permittivity studies show the decrease in relative permittivity of the ferrite material.
Keywords:
Nanomaterials Sol-Gel, XRD, SEM Relative Permittivity.
References:
[1] V. Naidu et al., "Synthesis and Characterization of Novel Nanoceramic Magnesium Ferrite Material Doped with Samarium and Dysprosium for Designing – Microstrip Patch Antenna", Defect and Diffusion Forum, Vol. 332, pp. 35-50, 2012
[2] S.K.A.Ahamed Kandu Sahib , M.Suganthi , Vasant Naidu , S.Pandian and M.Sivabharathy, ―Electrical and Magnetic properties of ZNCF‖, International Journal of Chem Tech Research CODEN (USA): IJCRGG ISSN : 0974-4290 Vol.6, No.11, pp 4615-4624, Oct-Nov 2014
[3] S.K.A.Ahamed Kandu Sahib , et al ―Synthesis Of Double Lanthanide Doped Nano Ferrite Meta Material For Microstrip Patch Antenna‖ Application International Journal of ChemTech Research CODEN (USA): IJCRGG ISSN : 0974-4290 Vol.6, No.11, pp 4615-4624, Oct-Nov 2014
[4] S.K.A.Ahamed Kandu Sahib , Vasant Naidu S. Amalorpava Mary Rajee S. Vijay Anand, ―Magnetic Property Study of Nickel Cerium Doped Zinc Ferrite Nano Particles‖, International Journal of Computer Applications (0975 – 8887) Volume 40– No.4, February 2012,
[5] Vasant Naidu, et. al , “Mg Sm Ferrite for Nano structured EShaped Patch Antenna studies‖, International Journal of Computer Applications (0975 – 8887) Volume 30– No.5, September 2011,
[6] S.K.A. Ahamed Kandu Sahib , et al., ―Design and Fabrication of Triangular Shape Microstrip Patch Antenna" Using Lanthanides‖ International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056 Volume: 04 Issue: 04 | Apr -2017 www.irjet.net p-ISSN: 2395-0072
[7] Vasant Naidu, et.al , “Magnetic properties of Nickel, Samarium doped Zinc ferrite, International Journal of Computer Applications”, 24[2] (2011), 18-22.
[8] A. Pradeep, P .Priyadharsini, G.Chandrasekaran., ―Sol-gel route of nano particles of MgFe2O4 and XRD,FTIR and VSM study‖, [J] Journal of Magn. Mag. Mater, 2008, 320, 2779.
[9] U.Ozgur, Y.Alivov, and H.M orkoç, “Microwave Ferrites, Part 1: Fundamental Properties”, [J] J. M ter. Sci.: Materials in Electronics”, 2009, 1-169.
[10] L.B Kong., et.al, “Magneto-Dielectric Properties of Mg-Cu- Co Ferrite Ceramics: II Electrical, Dielectric, and Magnetic Properties”, [J] J. Am. Ceram. Soc., 2007, 7, 2104-2112.
[11] E.M Elagiriyappa, H.S Jayanna, B.K.Chougule., ―Dielectric behavior and ac electrical conductivity study of Sm3+ substituted Mg-Zn ferrites‖ , [J] Journal of M aterials Chemistry and Physics, 2008 , 112 , pp 68-73.
[12] Vasant Naidu..et.al , ―Magnetic properties of Nickel, Cerium doped Zinc ferrite”, International Journal of Computer Applications (0975 – 8887),2011.
[13] Wilhelm Van Aulock (Ed.), [M] Handbook of microwaves ferrites Materials Academic Press,Newyork,London,1965.
[14] O.S. Josyulu, J. Shobanadri , [M ] Phy . Status Sol. , 1980, 59, 323.
[15] V.R.K. Murthy, J.Shobanadri, [M ] Phy .Status Sol., 1976, 36 , 133
[16] M .L. Khan and Z.J. Zhang, [J] Appl. Phys. Lett., 2001, 78, 3651.
[17] A.A Sattar.., et.al, Rare Earth Doping Effect on the Electrical Properties of Cu-Zn Ferrites, [J] J. Phys. IV France 1997.