Silver Nano Particle-Containing Inorganic–Organic Hybrid via Sol–Gel Synthesis

International Journal of Applied Chemistry

© 2018 by SSRG - IJAC Journal

Volume 5 Issue 1

Year of Publication : 2018

Authors : Ming-Shien Yen

10.14445/23939133/IJAC-V5I1P105

How to Cite?

Ming-Shien Yen, "Silver Nano Particle-Containing Inorganic–Organic Hybrid via Sol–Gel Synthesis," SSRG International Journal of Applied Chemistry, vol. 5,  no. 1, pp. 22-28, 2018. Crossref, https://doi.org/10.14445/23939133/IJAC-V5I1P105

Abstract:

Inorganic–organic hybrids containing silver nanoparticles (Ag NPs) were synthesized with silica and thiazole azo dye by a sol–gel process using vinyltriethoxysilane (VTES) as a precursor. The materials were synthesized from tetraethoxysilane (TEOS) with thiazole azo dyes, which in turn were synthesized using 2-amino thiazole as the coupling component that underwent a coupling reaction with the diazonium component, p-nitroaniline. Alternatively, the thiazole azo dyes were processed by the hydrolysis-condensation reaction with constant ratios of VTES and TEOS in appropriate proportions using a catalyst, followed by the incorporation of various ratios of Ag NPs. The structures of these hybrid materials were examined by Fourier transform infrared analysis, 29Si nuclear magnetic resonance spectroscopy, X-ray diffraction, and energy-dispersive X-ray spectroscopy.

Keywords:

Ag NPs, silica, thiazole dyes, hybrid materials

References:

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